ACQUITY UPLC BEH苯基柱含有一个三键键合的苯己基配体，与其他苯基色谱柱相比，它提供了行业的pH稳定性、批次重现性和优异的峰形。它设计用于提供相对于直链烷烃柱互补的选择性，特别是对于那些含有芳香环的分析物。
Simultaneous determination of 12 illicit drugs in whole blood and urine by solid phase extraction and UPLC–MS/MS
A rapid and sensitive method based on solid phase extraction and ultra performance liquid chromatography–electrospray ionization tandem mass spectrometry (UPLC–ESI-MS/MS) for the simultaneous determination of amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine, 3,4-methylene-dioxymethamphetamine, N-methyl-1-(3,4-methyl-enedioxyphenyl)-2-butanamine, 3,4-methylenedioxyethylamphetamine, p-methoxymethamphetamine, ephedrine, N-methylephedrine, cathinone, methcathinone, and ketamine in whole blood and urine was developed and validated. Following solid phase extraction, the analytes were separated on ACQUITY UPLC BEH Phenyl column (100 mm × 2.1 mm, 1.7 μm) under gradient elution using a phase containing of acetonitrile and 0.3% formic acid in water at a flow rate of 0.4 mL min−1 and analyzed by a triplequadrupole mass spectrometer in the multiple reaction monitoring (MRM) mode. The proposed method was linear for each analyte with correlation coefficients over 0.99. Recovery validation studies showed accuracy bias below 4.4%. Acceptable precision was also obtained with a relative standard deviation below 8.9%. The sensitivity of the assay was found to be adequate for the quantitation of the illicit drugs in whole blood and urine sample and was higher than reported methods. The present method was proved to be reliable and robust for drug screening in forensic toxicological analysis.
品名 | 编号 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 100 mm, 3/pkg | 176000908 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 1 mm X 150 mm, 3/pkg | 176001047 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 150 mm, 1/pkg | 186003378 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 1 mm X 100 mm, 1/pkg | 186002883 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 150 mm, 3/pkg | 176001051 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 100 mm, 1/pkg | 186002885 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 30 mm, 1/pkg | 186003911 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 1 mm X 50 mm, 3/pkg | 176000905 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 1 mm X 100 mm, 3/pkg | 176000906 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 1 mm X 50 mm, 1/pkg | 186002882 |
ACQUITY UPLC BEH Phenyl Method Validation Kit, 130Å, 1.7 µm, 2.1 mm X 100 mm, 3/pkg | 186004052 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 75 mm, 1/pkg | 186005607 |
ACQUITY UPLC BEH Phenyl Method Validation Kit, 130Å, 1.7 µm, 2.1 mm X 50 mm, 3/pkg | 186004050 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 50 mm, 3/pkg | 176000907 |
ACQUITY UPLC BEH Phenyl Method Validation Kit, 130Å, 1.7 µm, 2.1 mm X 150 mm, 3/pkg | 186006022 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 150 mm, 3/pkg | 176001809 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 30 mm, 3/pkg | 176001311 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 50 mm, 3/pkg | 176001807 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 100 mm, 3/pkg | 176001808 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 30 mm, 3/pkg | 176001806 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 75 mm, 1/pkg | 186005612 |
ACQUITY UPLC BEH Phenyl Method Validation Kit, 130Å, 1.7 µm, 3 mm X 100 mm, 3/pkg | 186004698 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 2.1 mm X 50 mm, 1/pkg | 186002884 |
ACQUITY UPLC BEH Phenyl VanGuard Pre-column, 130Å, 1.7 µm, 2.1 mm X 5 mm, 3/pkg | 186003979 |
ACQUITY UPLC BEH Phenyl Method Validation Kit, 130Å, 1.7 µm, 3 mm X 50 mm, 3/pkg | 186004697 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 30 mm, 1/pkg | 186004671 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 150 mm, 1/pkg | 186004674 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 50 mm, 1/pkg | 186004672 |
ACQUITY UPLC BEH Phenyl Column, 130Å, 1.7 µm, 3 mm X 100 mm, 1/pkg | 186004673 |
